Synthesis of thiocarbohydrazide and carbohydrazide derivatives as possible biologically active agents
Identifieur interne : 001223 ( Main/Exploration ); précédent : 001222; suivant : 001224Synthesis of thiocarbohydrazide and carbohydrazide derivatives as possible biologically active agents
Auteurs : Kiran Gangarapu [Inde] ; Sarangapani Manda ; Anvesh Jallapally ; Sreekanth Thota [États-Unis] ; Subhas S. Karki ; Jan Balzarini [Belgique] ; Erik De Clercq [Belgique] ; Harukuni Tokuda [Japon]Source :
- Medicinal Chemistry Research [ 1054-2523 ] ; 2013.
Abstract
A series of new β-isatin aldehyde-
Url:
DOI: 10.1007/s00044-013-0684-3
PubMed: NONE
PubMed Central: 7080202
Affiliations:
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id="Aff5"><institution-wrap><institution-id institution-id-type="GRID">grid.47894.36</institution-id><institution-id institution-id-type="ISNI">0000000419368083</institution-id><institution>Department of Chemistry,</institution><institution>Colorado State University,</institution></institution-wrap>Fort Collins, 80523 CO USA</nlm:aff><country>États-Unis</country><placeName><region type="state">Colorado</region></placeName><wicri:regionArea>Fort Collins</wicri:regionArea></affiliation></author><author><name sortKey="Karki, Subhas S" sort="Karki, Subhas S" uniqKey="Karki S" first="Subhas S." last="Karki">Subhas S. Karki</name><affiliation><nlm:aff id="Aff6"><institution-wrap><institution-id institution-id-type="GRID">grid.411053.2</institution-id><institution-id institution-id-type="ISNI">0000 0001 1889 7360</institution-id><institution>Department of Pharmaceutical Chemistry,</institution><institution>KLE University’s College of Pharmacy,</institution></institution-wrap>Rajajinagar, Bangalore, KN India</nlm:aff><wicri:noCountry code="subfield">KN India</wicri:noCountry></affiliation></author><author><name sortKey="Balzarini, Jan" sort="Balzarini, Jan" uniqKey="Balzarini J" first="Jan" last="Balzarini">Jan Balzarini</name><affiliation wicri:level="1"><nlm:aff id="Aff7"><institution-wrap><institution-id institution-id-type="GRID">grid.415751.3</institution-id><institution>Rega Institute for Medical Research, KU Leuven,</institution></institution-wrap>Leuven, Belgium</nlm:aff><country xml:lang="fr">Belgique</country><wicri:regionArea>Leuven</wicri:regionArea></affiliation></author><author><name sortKey="De Clercq, Erik" sort="De Clercq, Erik" uniqKey="De Clercq E" first="Erik" last="De Clercq">Erik De Clercq</name><affiliation wicri:level="1"><nlm:aff id="Aff7"><institution-wrap><institution-id institution-id-type="GRID">grid.415751.3</institution-id><institution>Rega Institute for Medical Research, KU Leuven,</institution></institution-wrap>Leuven, Belgium</nlm:aff><country xml:lang="fr">Belgique</country><wicri:regionArea>Leuven</wicri:regionArea></affiliation></author><author><name sortKey="Tokuda, Harukuni" sort="Tokuda, Harukuni" uniqKey="Tokuda H" first="Harukuni" last="Tokuda">Harukuni Tokuda</name><affiliation wicri:level="1"><nlm:aff id="Aff8"><institution-wrap><institution-id institution-id-type="GRID">grid.9707.9</institution-id><institution-id institution-id-type="ISNI">0000000123083329</institution-id><institution>Department of Complementary and Alternative Medicine,</institution><institution>Clinical R&D, Graduate School of Medical Science Kanazawa University,</institution></institution-wrap>Kanazawa, Japan</nlm:aff><country xml:lang="fr">Japon</country><wicri:regionArea>Kanazawa</wicri:regionArea></affiliation></author></analytic><series><title level="j">Medicinal Chemistry Research</title><idno type="ISSN">1054-2523</idno><idno type="eISSN">1554-8120</idno><imprint><date when="2013">2013</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><sec><title>Abstract</title><p>A series of new β-isatin aldehyde-<italic>N</italic>,<italic>N</italic>′-thiocarbohydrazone, bis-β-isatin thiocarbohydrazones, bis-β-isatin carbohydrazones was synthesized by condensation of 5-substituted isatin with thiocarbohydrazide or carbohydrazide. The chemical structures of the newly synthesized compounds were confirmed by FT-IR, <sup>1</sup>H NMR, and mass spectral analysis. The synthesized compounds were evaluated for in vitro antiviral activity against various strains of DNA and RNA viruses, but exhibited moderate antiviral activity compared with the reference compounds. Among all the compounds <bold>6c</bold> exhibited the highest chemoprevention activity in a two-stage mouse-skin carcinogenesis test.</p></sec><sec><title>Graphical abstract</title><p><graphic position="anchor" xlink:href="44_2013_684_Figa_HTML" id="MO1"></graphic></p></sec></div></front><back><div1 type="bibliography"><listBibl><biblStruct><analytic><author><name sortKey="Akhaja, Tn" uniqKey="Akhaja T">TN Akhaja</name></author><author><name sortKey="Raval, Jp" uniqKey="Raval J">JP Raval</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Alcaide, B" uniqKey="Alcaide B">B Alcaide</name></author><author><name sortKey="Almendros, P" uniqKey="Almendros P">P Almendros</name></author><author><name sortKey="Aragoncillo, C" uniqKey="Aragoncillo C">C Aragoncillo</name></author><author><name sortKey="Campillos, Gg" uniqKey="Campillos G">GG Campillos</name></author><author><name sortKey="Arn, M" uniqKey="Arn M">M Arnó</name></author><author><name sortKey="Domingo, Lr" uniqKey="Domingo L">LR Domingo</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Bacani, Pmc" uniqKey="Bacani P">PMC Bacani</name></author><author><name sortKey="Reis, Mb" uniqKey="Reis M">MB Reis</name></author><author><name sortKey="Serpeloni, Jm" uniqKey="Serpeloni J">JM Serpeloni</name></author><author><name sortKey="Calvo, Tr" uniqKey="Calvo T">TR Calvo</name></author><author><name sortKey="Vilegas, W" uniqKey="Vilegas W">W Vilegas</name></author><author><name sortKey="Varanda, Ea" uniqKey="Varanda E">EA Varanda</name></author><author><name sortKey="C Lus, Ims" uniqKey="C Lus I">IMS Cólus</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Bal, Tr" uniqKey="Bal T">TR Bal</name></author><author><name sortKey="Anand, B" uniqKey="Anand B">B Anand</name></author><author><name sortKey="Yogeeswari, P" uniqKey="Yogeeswari P">P Yogeeswari</name></author><author><name sortKey="Sriram, D" uniqKey="Sriram D">D 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Thuring</name></author><author><name sortKey="Wang, Xa" uniqKey="Wang X">XA Wang</name></author><author><name sortKey="Yang, Z" uniqKey="Yang Z">Z Yang</name></author><author><name sortKey="Zadjura, L" uniqKey="Zadjura L">L Zadjura</name></author><author><name sortKey="Marino, A" uniqKey="Marino A">A Marino</name></author><author><name sortKey="Kadow, Kf" uniqKey="Kadow K">KF Kadow</name></author><author><name sortKey="Cianci, Cw" uniqKey="Cianci C">CW Cianci</name></author><author><name sortKey="Clarke, J" uniqKey="Clarke J">J Clarke</name></author><author><name sortKey="Genovesi, Esv" uniqKey="Genovesi E">ESV Genovesi</name></author><author><name sortKey="Medina, I" uniqKey="Medina I">I Medina</name></author><author><name sortKey="Lamb, L" uniqKey="Lamb L">L Lamb</name></author><author><name sortKey="Krystal, M" uniqKey="Krystal M">M Krystal</name></author><author><name sortKey="Meanwell, Na" uniqKey="Meanwell N">NA Meanwell</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Tanaka, R" uniqKey="Tanaka R">R Tanaka</name></author><author><name sortKey="Minami, T" uniqKey="Minami T">T Minami</name></author><author><name sortKey="Tsujimoto, K" uniqKey="Tsujimoto K">K Tsujimoto</name></author><author><name sortKey="Matsunga, S" uniqKey="Matsunga S">S Matsunga</name></author><author><name sortKey="Tokuda, H" uniqKey="Tokuda H">H Tokuda</name></author><author><name sortKey="Nishino, H" uniqKey="Nishino H">H Nishino</name></author><author><name sortKey="Terada, Y" uniqKey="Terada Y">Y Terada</name></author><author><name sortKey="Yoshitake, A" uniqKey="Yoshitake A">A Yoshitake</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Teitz, Y" uniqKey="Teitz Y">Y Teitz</name></author><author><name sortKey="Ronen, D" uniqKey="Ronen D">D Ronen</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Zhou, J" uniqKey="Zhou J">J Zhou</name></author><author><name sortKey="Wu, D" uniqKey="Wu D">D Wu</name></author><author><name sortKey="Gou, J" uniqKey="Gou J">J Gou</name></author></analytic></biblStruct></listBibl></div1></back></TEI><affiliations><list><country><li>Belgique</li><li>Inde</li><li>Japon</li><li>États-Unis</li></country><region><li>Colorado</li></region></list><tree><noCountry><name sortKey="Jallapally, Anvesh" sort="Jallapally, Anvesh" uniqKey="Jallapally A" first="Anvesh" last="Jallapally">Anvesh Jallapally</name><name sortKey="Karki, Subhas S" sort="Karki, Subhas S" uniqKey="Karki S" first="Subhas S." last="Karki">Subhas S. Karki</name><name sortKey="Manda, Sarangapani" sort="Manda, Sarangapani" uniqKey="Manda S" first="Sarangapani" last="Manda">Sarangapani Manda</name></noCountry><country name="Inde"><noRegion><name sortKey="Gangarapu, Kiran" sort="Gangarapu, Kiran" uniqKey="Gangarapu K" first="Kiran" last="Gangarapu">Kiran Gangarapu</name></noRegion></country><country name="États-Unis"><region name="Colorado"><name sortKey="Thota, Sreekanth" sort="Thota, Sreekanth" uniqKey="Thota S" first="Sreekanth" last="Thota">Sreekanth Thota</name></region></country><country name="Belgique"><noRegion><name sortKey="Balzarini, Jan" sort="Balzarini, Jan" uniqKey="Balzarini J" first="Jan" last="Balzarini">Jan Balzarini</name></noRegion><name sortKey="De Clercq, Erik" sort="De Clercq, Erik" uniqKey="De Clercq E" first="Erik" last="De Clercq">Erik De Clercq</name></country><country name="Japon"><noRegion><name sortKey="Tokuda, Harukuni" sort="Tokuda, Harukuni" uniqKey="Tokuda H" first="Harukuni" last="Tokuda">Harukuni Tokuda</name></noRegion></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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